Methyl iodide → HCID 19075355, compound

HRID 744659Notes

Reaction equation

HRID 744659 reaction equation
[CH3:1][I:2].[O:3]1[CH2:8][CH2:7][N:6]([C:9]2[C:10]([C:14]3[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=3)=[N:11][S:12][N:13]=2)[CH2:5][CH2:4]1>CC(C)=O>[I-:2].[O:3]1[CH2:4][CH2:5][N:6]([C:9]2[C:10]([C:14]3[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=3)=[N:11][S:12][N:13]=2)[CH2:7][CH2:8]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075225HCID 19075225, compound

Product 1

HCID 19075355HCID 19075355, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(4-morpholino-1,2,5-thiadiazol-3-yl )pyridine (680 mg, 2.7 mmol ) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 1.0 g (94%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 1.0 g (94%)

Sources & evidence

ORD record
ord-2bb97f41c24345fb8bfaf813eaa5d69a
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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