Methyl iodide → HCID 19075210, compound

HRID 744661Notes

Reaction equation

HRID 744661 reaction equation
[CH3:1][I:2].[CH2:3]([NH:9][C:10]1[C:11]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([NH:9][C:10]1[C:11]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180169HCID 15180169, compound

Product 1

HCID 19075210HCID 19075210, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.6 ml, 9.6 mmol) and 3-(4-hexylamino-1,2,5-thiadiazol-3-yl )pyridine (3.2 mmol) in acetone (5 ml) was stirred at room temperature for 18 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-0d6dedc617fc498baac3c0fb3edc6f1b
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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