Methyl iodide → HCID 19075292, compound

HRID 744667Notes

Reaction equation

HRID 744667 reaction equation
[CH3:1][I:2].[CH3:3][S:4][C:5]1[C:6]([C:10]2[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=2)=[N:7][S:8][N:9]=1>>[I-:2].[CH3:3][S:4][C:5]1[C:6]([C:10]2[CH:11]=[N+:12]([CH3:1])[CH:13]=[CH:14][CH:15]=2)=[N:7][S:8][N:9]=1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 15180153HCID 15180153, compound

Product 1

HCID 19075292HCID 19075292, compound

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(4-methylthio-1,2,5-thiadiazol-3-yl)pyridine (0.5 g, 2.3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-b52c3a42bc354d79b7e700a10c991036
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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