Methyl iodide → HCID 19075279, compound

HRID 744672Notes

Reaction equation

HRID 744672 reaction equation
[CH3:1][I:2].[Cl:3][C:4]1[C:5]([C:9]2[CH:10]=[N:11][CH:12]=[CH:13][CH:14]=2)=[N:6][O:7][N:8]=1>CC(C)=O>[I-:2].[Cl:3][C:4]1[C:5]([C:9]2[CH:10]=[N+:11]([CH3:1])[CH:12]=[CH:13][CH:14]=2)=[N:6][O:7][N:8]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180172HCID 15180172, compound

Product 1

HCID 19075279HCID 19075279, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(4-chloro-1,2,5-oxadiazol-3-yl)pyridine (230 mg, 1.2 mmol) in acetone. The reaction mixture was stirred at room temperature for 18 h and evaporated to give the title compound.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-65457ac2166e4857a9cee7b61477f1c2
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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