Methyl iodide → HCID 19075222, compound

HRID 744673Notes

Reaction equation

HRID 744673 reaction equation
[CH3:1][I:2].[O:3]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=2)=[N:4]1>CC(C)=O>[I-:2].[O:3]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[N+:10]([CH3:1])[CH:11]=[CH:12][CH:13]=2)=[N:4]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075301HCID 19075301, compound

Product 1

HCID 19075222HCID 19075222, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(1,2,5-oxadiazol-3-yl)pyridine (430 mg, 2.9 mmol) in acetone (20 ml). The reaction mixture was stirred at room temperature for 18 h. The product precipitated from the solution and the title compound was collected by filtration in 82% (700 mg) yield.

Workup

  1. customThe product precipitated from the solution
  2. filtrationthe title compound was collected by filtration in 82% (700 mg)
  3. customyield

Sources & evidence

ORD record
ord-fa9f8a0edeb048c9b10d57db910ddc27
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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