Methyl iodide → 3-(3-(5-Cyanopentylthio)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

HRID 744730Notes

Reaction equation

HRID 744730 reaction equation
[CH3:1][I:2].[C:3]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][S:10][C:11]1[C:15]([C:16]2[CH:17]=[N:18][CH:19]=[CH:20][CH:21]=2)=[N:14][S:13][N:12]=1)#[N:4]>CC(C)=O>[I-:2].[C:3]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][S:10][C:11]1[C:15]([C:16]2[CH:17]=[N+:18]([CH3:1])[CH:19]=[CH:20][CH:21]=2)=[N:14][S:13][N:12]=1)#[N:4]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 196125283-(3-(5-Cyanopentylthio)-1,2,5-thiadiazol-4-yl)pyridine

Product 1

HCID 196125523-(3-(5-Cyanopentylthio)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-(5-cyanopentylthio)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone and the reaction mixture was stirred at room temperature for 20 h. and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-63bcc91c2b4d431fa842a435d556b1b9
Source dataset
uspto-grants-1996_09
Patent number
US05559136

Reaction notes

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