HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 23369935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | Benzyl 4-(ethylamino)piperidine-1-carboxylate | HCID 23369962 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 23369935 | HCID 23369935 | — |
Reaction Steps
A solution of 1-benzyloxycarbonyl-4-(N-ethylamino)piperidine (4.0 g) and methyl isocyanate (11 mL) was stirred for 30 hours at ambient temperature. The reaction mixture was diluted with chloroform and evaporated to give the urea as an oil; MS: m/z=320(M+1). The material was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559131 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-97d4136638db4e0dbf40e618a0094654 |
| Source note | uspto-grants-1996_09 |