HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[4-(dimethylamino)phenyl]-2-phenylethane-1,2-dione → HCID 13236224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[4-(dimethylamino)phenyl]-2-phenylethane-1,2-dione | HCID 231231 | — |
| Reactant | 2-Cyanoethanethioamide | HCID 1416277 | — |
| Catalyst | Piperidine | HCID 8082 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13236224 | HCID 13236224 | — |
Reaction Steps
A mixture of 10.1 g. p-dimethylaminobenzil, 3.2 g. cyanothioacetamide, 10 drops of piperidine and 100 ml. ethanol is stirred for 12 hours at ambient temperature. The precipitated product is filtered off with suction, washed with chloroform and recrystallised from ethanol. There are obtained 6.0 g. of the desired product in the form of yellow crystals; m.p. 184°-185° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04598076 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-f2aa5cfe40e14b00a6f7168c3c021f81 |
| Source note | uspto-grants-1986_07 |