HCID 70472814, compound → Benzenecarboximidamide, 4-(2-(4-(aminomethyl)phenyl)ethyl)-, dihydrochloride

Participants

Reaction Steps

A solution of 30 mg of 4-[2-(4-aminomethylphenyl)ethenyl]benzamidine dihydrochloride in 30 ml of methanol was catalytically reduced with 20 mg of a 5% palladium-carbon as catalyst. The reaction mixture was filtered from spent catalyst and concentrated under reduced pressure. The residue was recrystallized from a methanolisopropanol-ether mixture to yield 20 mg of 4-[2-(4-aminomethylphenyl)ethyl]benzamidine dihydrochloride; m.p. ≥260° C.

Provenance & Evidence