Triphenylphosphine → HCID 86740883, compound

Participants

Reaction Conditions

Reaction Steps

Into a 500 ml, three-necked, round-bottom flask equipped with a reflux condenser, a magnetic stir bar, and a static argon inlet, was placed 5.90 g (24 mmol) of the 1-bromo-4,8,12-trimethyltridecane and 6.64 g (25 mmol) of triphenylphosphine. The resulting mixture was stirred in an oil bath at 180° C. overnight (19 hours). The resulting phosphonium salt, i.e. 4,8,12-trimethyltridecyl, was used without further purification or storage.

Provenance & Evidence