HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → Ethyl 2-benzyloxyimino-4-chloro-3-oxobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | Ethyl 2-benzyloxyimino-3-oxobutyrate | HCID 53396355 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Ethyl 2-benzyloxyimino-4-chloro-3-oxobutyrate | HCID 53794160 | 85.7% |
Reaction Steps
A solution of ethyl 2-benzyloxyimino-3-oxobutyrate (syn isomer, 56.0 g.), sulfuryl chloride (40.5 g.) and acetic acid (80 ml.) was treated in a similar manner to that of Example A-(2) to give ethyl 2-benzyloxyimino-4-chloro-3-oxobutyrate (syn isomer, 54.6 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04598147 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-8f1beda3431f4ab7aafc597aedfbd42c |
| Source note | uspto-grants-1986_07 |