HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23315738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | alpha,alpha'-Dichloro-p-xylene | HCID 12171 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 23315738 | HCID 23315738 | 59.2% |
Reaction Steps
A mixture of 1,4-bis(chloromethyl)benzene (25 g.), N-hydroxyphthalimide (23.4 g.) and triethylamine (14.5 g.) in acetonitrile (200 ml.) was heated under reflux for 1.5 hours. The reaction mixture was poured into ice-water (1 l.) and the precipitates were collected by filtration. The precipitates were washed with ethanol and dried to give N-(4-chloromethylbenzyloxy)phthalimide (25.5 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04598147 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-7a1577f663294bbcb3c15a439b5140ee |
| Source note | uspto-grants-1986_07 |