HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → Diethyl 2-phenylethyl phosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Product | Diethyl 2-phenylethyl phosphonate | HCID 3448525 | — |
Reaction Steps
In a manner according to Preparation 2 combine 2-phenylethyl bromide and triethyl phosphite. Distill the mixture at reduced pressure (0.15 mm Hg) and collect the fraction distilling at 115°-130° C. to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04599344 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-5fdc8f3c0f904a119539b199c5f50e6d |
| Source note | uspto-grants-1986_07 |