1-Bromoheptane → HCID 23313720, compound

HRID 745552Notes

Reaction equation

[O:1]=[C:2]1[CH:7]2[CH2:8][CH2:9][N:4]([CH2:5][CH2:6]2)[CH:3]1[CH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19][S:20]([CH3:23])(=[O:22])=[O:21])=[CH:15][CH:14]=1.[CH2:24]([Br:31])[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]>>[Br-:31].[CH2:24]([N+:4]12[CH2:9][CH2:8][CH:7]([CH2:6][CH2:5]1)[C:2](=[O:1])[CH:3]2[CH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19][S:20]([CH3:23])(=[O:22])=[O:21])=[CH:15][CH:14]=1)[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]

Participants

Reactant 2

HCID 123691-Bromoheptane

HCID 23313742HCID 23313742, compound

Product 1

HCID 23313720HCID 23313720, compound

Procedure

In a manner similar to Example II, Method A, react N-[4-(3-(3-oxo-1-azabicyclo[2.2.2]oct-2-yl)propyl)phenyl]-methanesulfonamide with heptyl bromide to yield the title compound.

Sources & evidence

ORD record: ord-bd9e909ed3934c14be7e2475ef75f4be
Source dataset: uspto-grants-1986_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04599344

Reaction notes

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