2-Methylene-3-quinuclidone → HCID 23313755, compound

HRID 745559Notes

Reaction equation

HRID 745559 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:13])[CH2:9][C:10](=[O:12])[CH3:11])=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].[CH2:17]=[C:18]1[C:23](=[O:24])[CH:22]2[CH2:25][CH2:26][N:19]1[CH2:20][CH2:21]2>CC(C)=O>[ClH:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:13])[CH:9]([CH2:17][CH:18]2[C:23](=[O:24])[CH:22]3[CH2:25][CH2:26][N:19]2[CH2:20][CH2:21]3)[C:10](=[O:12])[CH3:11])=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15]

Participants

4

Reactant 2

HCID 3229732-Methylene-3-quinuclidoneHCID 23313726HCID 23313726, compound

Product 1

HCID 23313755HCID 23313755, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

In a manner similar to Example XXV react 1-(4-chloro-3-nitrophenyl)-1,3-butanedione with 2-methylene-3-quinuclidinone in acetone to provide the title compound.

Sources & evidence

ORD record
ord-932f1e7448c84d699178fcc37c3f263b
Source dataset
uspto-grants-1986_07
Patent number
US04599344

Reaction notes

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