HRID745624

反应详情

EQUATION

反应方程式

HRID 745624 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

E and Z benzyl 3-(ethoxycarbonyl)-2-(2-methylpropyl)butenoate (5.0 g.) was hydrogenated at 120 psi at 60° C. in methanol (50 mls.) in the presence of 10% palladium on charcoal (0.25 g.) for 48 hours. The resultant mixture was filtered through Celite and the solvent removed by evaporation in vacuo to yield 3-(ethoxycarbonyl)-2-(2-methylpropyl)butanoic acid as a mixture of isomers in the form of a thick oil.

WORKUP

后处理

  1. filtrationThe resultant mixture was filtered through Celite
  2. customthe solvent removed by evaporation in vacuo