Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3,3-Difluoro-4-methylpentane-1,4-diol | HCID 13189246 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13248173 | HCID 13248173 | — |
Reaction Steps
To a mixture of 6.92 g (0.045 mol) of 4-methyl-3,3-difluoro-1,4-pentanediol and 28 mL of pyridine at 0° C. was added 16 mL of acetic anhydride and the mixture was stirred at 0° C. for 1 hr and at 25° C. for 1 hr. The mixture was added to 15 mL of methanol and the solution was evaporated to dryness to yield oily 4-methyl-3,3-difluoro-1,4-pentanediol 1-acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04599330 |
|---|
| Source dataset | uspto-grants-1986_07 |
|---|
| ORD ID | ord-5c09a861239a461d85f334aff0bd2d7a |
|---|
| Source note | uspto-grants-1986_07 |
|---|
