HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → Piperazine, phosphate (1:?)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | Phosphate | HCID 1061 | — |
| Reactant | Piperazine | HCID 4837 | — |
| Solvent | Water | HCID 962 | — |
| Product | Piperazine, phosphate (1:?) | HCID 64733 | — |
Reaction Steps
200 g of H3PO4 (85%) in 200 cc of H2O were reacted with 77 g of piperazine (97%) in 300 cc of H2O at a maximum temperature of 65° C. and at a pH of about 5. The precipitate, consisting of the acid orthophosphate of piperazine, was maintained at a temperature from 0° to 5° C. for about 20 hours, then it was filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04599375 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-0288dabf1c3f4df4aaad1ec45fe4a8c0 |
| Source note | uspto-grants-1986_07 |