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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 745767Generated: October 30, 2026

Dimethylformamide → HCID 54135768, compound

https://huagongshe.com/reaction/745767

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamideHCID 6228—
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 23312160HCID 23312160—
ProductHCID 54135768HCID 54135768—

Reaction Steps

590 mg of 3-ethoxycarbonyl-4-ethyl-β-carboline-6-carboxylic acid is refluxed in 6 ml of thionyl chloride with a drop of dimethylformamide for 2.5 hours. After evaporation and drying, 664 mg of 3-ethoxycarbonyl-4-ethyl-β-carboline-6-carboxylic acid chloride is obtained in the form of the hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04600715
Source datasetuspto-grants-1986_07
ORD IDord-0ee6d66dc9e140c282294f4548b20b4c
Source noteuspto-grants-1986_07