HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 4-Chloro-5-(sulfamoyl)-1,2-benzenedicaboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-(Aminosulfonyl)-5-chlorophthalimide | HCID 19733 | — |
| Product | 4-Chloro-5-(sulfamoyl)-1,2-benzenedicaboxamide | HCID 13370599 | — |
Reaction Steps
A solution of 4-chloro-5-sulfamoylphthalimide (21.3 g., 0.076 mole) and 250 ml. of liquid ammonia was stirred at room temperature while permitting ammonia to evaporate. Water was added to residual material, the pH adjusted to 7 with hydrochloric acid and precipitated material collected to provide 14.5 g. (63%) of hydrated 4-chloro-5-(sulfamoyl)-1,2-benzenedicarboxamide, m.p. 270°-275° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04600758 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-01621d922c4a45f2b8e94e088ed30e71 |
| Source note | uspto-grants-1986_07 |