HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzoic acid, 2-(aminosulfonyl)-, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Saccharin | HCID 5143 | — |
| Product | Benzoic acid, 2-(aminosulfonyl)-, methyl ester | HCID 42546 | — |
Reaction Steps
An HCl stream is led under cooling into a suspension of 143.3 g (0.78 mol) in 600 ml absolute methanol until saturation. Subsequently the solution is refluxed yet two hours until the saccharine has gone completely into solution and the reaction has terminated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04601746 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-7682b66929384626b8eedbdba4fb52da |
| Source note | uspto-grants-1986_07 |