HCID 13656013, compound → HCID 13656014, compound
Reaction equation
[CH2:1]([CH:8]([CH2:14][C:15]#[C:16]C)[C:9]([O:11]CC)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:18](C(CC#CC)C(O)=O)C1C=CC=CC=1>>[CH2:1]([C:8]([CH3:18])([CH2:14][C:15]#[CH:16])[C:9]([OH:11])=[O:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
By replacing ethyl 2-benzyl-2-methyl-5-trimethylsilylpent-4-ynoate with ethyl 2-benzylhex-4-ynoate, 2-benzylhex-4-ynoic acid was prepared; IR: 3300-2500, 1710 cm-1.
Workup
- customwas prepared
Sources & evidence
- ORD record
- ord-6abf9abcbb4441f2b2b7bf43074e1ade
- Source dataset
- uspto-grants-1986_07
- Patent number
- US04602006
Reaction notes
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