Cyanamide → HCID 178512391, compound

HRID 745928Notes

Reaction equation

HRID 745928 reaction equation
[C:1]([C:4]1[CH:17]=[CH:16][C:7]([O:8][CH2:9][CH2:10][N:11]2[CH:15]=[CH:14][N:13]=[CH:12]2)=[CH:6][CH:5]=1)([OH:3])=O.[N:18]#[C:19][NH2:20]>>[C:19]([N:20]=[C:1]([C:4]1[CH:17]=[CH:16][C:7]([O:8][CH2:9][CH2:10][N:11]2[CH:15]=[CH:14][N:13]=[CH:12]2)=[CH:6][CH:5]=1)[OH:3])#[N:18]

Participants

3

Reactant 2

HCID 9864CyanamideHCID 53001Dazoxiben

Product 1

HCID 178512391HCID 178512391, compound

Procedure

Treatment of 1-[2-(4-carboxyphenoxy)ethyl]imidazole with N,N'-carbonyldiimidazole followed by cyanamide as described in Example 36 above gave N-cyano-4-[2-(1-imidazolyl)ethoxy]benzenecarboximidic acid, m.p. 199°-200° C. (d) (from water). Found: C, 60.59; H, 4.64; N, 22.20. C13H12N4O2 requires: C, 60.93; H, 4.72; N, 21.87%.

Sources & evidence

ORD record
ord-562b739df311405194089a0106418440
Source dataset
uspto-grants-1986_07
Patent number
US04602016

Reaction notes

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