Dimethylamine → HCID 23311190, compound

HRID 745933Notes

Reaction equation

HRID 745933 reaction equation
[CH3:1][C:2]1([CH2:21][CH2:22][CH2:23][CH3:24])[C:6]2[CH:7]=[N:8][C:9]([CH2:19]Cl)=[C:10]([O:11]CC3C=CC=CC=3)[C:5]=2[CH2:4][O:3]1.[CH3:25][NH:26][CH3:27]>C1C=CC=CC=1>[CH3:1][C:2]1([CH2:21][CH2:22][CH2:23][CH3:24])[C:6]2[CH:7]=[N:8][C:9]([CH2:19][N:26]([CH3:27])[CH3:25])=[C:10]([OH:11])[C:5]=2[CH2:4][O:3]1

Participants

4

Reactant 2

HCID 674DimethylamineHCID 23311185HCID 23311185, compound

Product 1

HCID 23311190HCID 23311190, compoundYield 48%

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The method of example 1 was repeated, but starting with 1,3-dihydro-3-methyl-3-n-butyl-6-chloromethyl-7-benzoxy-furo-(3,4-c)-pyridine and dimethylamine dissolved in benzene. Yield 48% of an oily product, elemental analysis of which showed a good correspondence with the formula C14H22N2O2.HCl.

Sources & evidence

ORD record
ord-7ae3bcc7fb954d688f36a62f02feb545
Source dataset
uspto-grants-1986_07
Patent number
US04602020

Reaction notes

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