m-Chloroperbenzoic acid → HCID 13688954, compound

Participants

Reaction Conditions

Reaction Steps

To 6.1 g (0.0143 mole) 3-(4-chlorophenylthio)-2-(2,4-dichlorobenzyloxy)-1-(1-imidazolyl)propane in methylene chloride (25 ml) at 0° C., 2.8 g (0.0143 mole) 85% meta-chloroperoxybenzoic acid in methylene chloride (50 ml) were added dropwise over about 30 minutes. The reaction mixture was maintained at about 0° C. during the addition and for about 11/2 to 2 hours after the addition. The reaction mixture was washed with a sodium bicarbonate solution (5%), with a bisulfite solution, dried, filtered, and concentrated to give 6.1 g of the above-identified product as a yellow oil.

Provenance & Evidence