4-Piperidinol, 1,2,2,6,6-pentamethyl- → HCID 23310771, compound
Reaction equation
[CH3:1][C:2]1[O:3][C:4]([CH3:12])=[C:5]([CH3:11])[C:6]=1[C:7]([O:9][CH3:10])=[O:8].OC1[CH2:19][C:18]([CH3:21])([CH3:20])[N:17]([CH3:22])[C:16]([CH3:24])([CH3:23])[CH2:15]1>>[CH3:1][C:2]1[O:3][C:4]([CH3:12])=[C:5]([CH3:11])[C:6]=1[C:7]([O:9][CH:10]1[CH2:19][C:18]([CH3:21])([CH3:20])[N:17]([CH3:22])[C:16]([CH3:24])([CH3:23])[CH2:15]1)=[O:8]Participants
3
Procedure
If methyl 2,4,5-trimethylfuran-3-carboxylate and 4-hydroxy-1,2,2,6,6-pentamethylpiperidine are reacted by the method given in Example 1, the product obtained is a virtually colorless oil of boiling point 138°-140° C./0.4 mm; this solidifies to a solid of melting point 55°-56° C.
Workup
- customthe product obtained
Sources & evidence
- ORD record
- ord-d887d440203a47b9a3142c46c81428bc
- Source dataset
- uspto-grants-1986_07
- Patent number
- US04603205
Reaction notes
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