Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2,4-Dichlorophenol | HCID 8449 | — |
| Reactant | 2,4-Dichloro-1-[(3,3-dimethylbut-1-yn-1-yl)oxy]benzene | HCID 13574877 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | HCID 13326123 | HCID 13326123 | — |
Reaction Steps
24.3 g (0.1 mole) of 1-(2,4-dichlorophenoxy)-3,3-dimethylbut-1-yne were initially taken together with 16.3 g (0.1 mole) of 2,4-dichlorophenol and 1.4 g (0.01 mole) of zinc chloride, and the stirred mixture was heated at 160° C. After 30 minutes, the phenol had reacted quantitatively with the phenoxyalkyne to give 1,1-bis-(2,4-dichlorophenoxy)-3,3-dimethylbut-1-ene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04603224 |
|---|
| Source dataset | uspto-grants-1986_07 |
|---|
| ORD ID | ord-befaf93dc49e4b73a850249b489e376d |
|---|
| Source note | uspto-grants-1986_07 |
|---|
