HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vanillin → 4-(allyloxy)-3-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vanillin | HCID 1183 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-(allyloxy)-3-methoxybenzaldehyde | HCID 2063823 | — |
Reaction Steps
Vanillin (20.0 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07393367B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-2262e4da654c4dfa925ae01a12cfcfdc |
| Source note | uspto-grants-2008_07 |