HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 4-(allyloxy)-3-ethoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Ethylvanillin | HCID 8467 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-(allyloxy)-3-ethoxybenzaldehyde | HCID 3525736 | — |
Reaction Steps
Ethyl vanillin (21.6 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07393367B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-90a5edfca4904f35b1b810a6754cd3bb |
| Source note | uspto-grants-2008_07 |