HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbazate → tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Reactant | 2-Quinolinecarboxaldehyde | HCID 79619 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate | HCID 69201455 | — |
Reaction Steps
A solution of 10.70 g 2-quinolinecarboxaldehyde and 9.00 g tert-butyl hydrazinecarboxylate in 200 ml of ethanol is refluxed for 2 h with stirring. Then the solution is evaporated to dryness and the residue is triturated with diisopropylether, separated off and dried at 50° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07393847B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-b0c24742b0534cffba3d932cbf487f85 |
| Source note | uspto-grants-2008_07 |