HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbazate → HCID 69201000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Reactant | Phenyl vinyl sulfone | HCID 79664 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69201000 | HCID 69201000 | — |
Reaction Steps
A solution of 0.79 g tert-butyl hydrazinecarboxylate and 1.00 g phenylvinylsulphone in 8 ml of ethanol is refluxed for 5 h with stirring. Then the solvent is removed completely and the residue is chromatographed over silica gel (cyclohexane/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07393847B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-10fbda7314014fd9af57ee8ed0823066 |
| Source note | uspto-grants-2008_07 |