Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfamic Acid | HCID 5987 | — |
| Reactant | HCID 21105701 | HCID 21105701 | — |
| Reactant | Sodium Chlorite | HCID 23668197 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21105702 | HCID 21105702 | — |
Reaction Steps
To a solution of 1-methoxy-6-acetamido dibenzo[b,d]thiophene-4-carbaldehyde (800 mg, 0.00266 mol) in THF (15 ml) and water (2 ml) was added sulfamic acid (387 mg, 0.004 mmol) while stirring at 10° C. A solution of 80% sodium chlorite (360 mg, 0.004 mmol) in water (2.0 mL) was added drop wise to the above reaction mixture over a period of 5 min
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07393846B2 |
|---|
| Source dataset | uspto-grants-2008_07 |
|---|
| ORD ID | ord-aefe157ac18f44bb862c83eff20b23b8 |
|---|
| Source note | uspto-grants-2008_07 |
|---|
