HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 23512715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 1-(8-Aminooctyl)-2-(2-methoxyethyl)-1H-imidazo[4,5-c]quinolin-4-amine | HCID 22344447 | — |
| Product | HCID 23512715 | HCID 23512715 | 44.6% |
Reaction Steps
Using the general method of Example 186 1-(8-aminooctyl)-2-(2-methoxyethyl)-1H-imidazo[4,5-c]quinolin-4-amine (0.84 g, 2.27 mmol) was reacted with benzoyl choride (260 μL, 2.27 mmol) to provide 0.48 g of N-{8-[4-amino-2-(2-methoxyethyl)-1H-imidazo[4,5-c]quinolin-1-yl]octyl}benzamide as a tan powder, m.p. 133.4-137.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07393859B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-a5698226388f44ea86eed5e61d9e30e0 |
| Source note | uspto-grants-2008_07 |