HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178418806, compound → HCID 178423809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178418806 | HCID 178418806 | — |
| Reactant | HCID 178423838 | HCID 178423838 | — |
| Reactant | HCID 178517101 | HCID 178517101 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178423809 | HCID 178423809 | — |
Reaction Steps
The named compound is prepared by substituting 5-(2,4-dimethyl-phenyl)-2H-pyrazol-3-ylamine for 3-aminopyrazole in the reaction of Example 1. Specifically, E & Z-3-[(hydroxy)-methylene]-1,3-dihydro-indol-2-one (0.100 gms.) is reacted with 0.250 gms. 5-(2,4-dimethyl-phenyl)-2H-pyrazol-3-ylamine by refluxing in tetrahydrofuran (2.0 mL) over the weekend.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07393870B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-8f08160b941a4612aadd2042eef621a7 |
| Source note | uspto-grants-2008_07 |