참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Carbethoxy-4-ethylamino-3-methylpiperidine | HCID 22278900 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | 4-Ethylamino-3-methylpiperidine | HCID 22278859 | — |
반응 단계
1-Carbethoxy-4-ethylamino-3-methylpiperidine (2.3 g, 10.74 mmol) was suspended in 5 M NaOH solution (15 ml), stirred at 110° C. for 120 hr, cooled, extracted with ethyl acetate, dried (Na2SO4) and concentrated to dryness to afford 4-ethylamino-3-methylpiperidine. Yield 0.7 g (46%), C8H18N2, m/z 143, (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07393957B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_07 |
|---|
| ORD ID | ord-310b5414d9e94fc88d6398a0075074e0 |
|---|
| 출처 메모 | uspto-grants-2008_07 |
|---|
