Hydrochloric Acid → HCID 67377193, compound

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Reaction Steps

The product obtained in example 68 (1 gm; 2.58 mmol) was suspended in 10 ml ethanol and ethanolic hydrochloric acid (2.6 ml) was added at a temperature between 20-30° C. under stirring. To this solution, 20 ml ether was added after 30 minutes and the solid separated was filtered and dried under vacuum. Yield −0.89 gm (83%). m.p. 242-244° C., C21H26FN3O3.HCl, m/z 388 (M+1).

Provenance & Evidence