反应详情

31.0 g of N,N-bis(2-cyanoethyl)hexylamine, 4.65 g of RaneyCo, 150 ml of 1,4-dioxane was charged to an autoclave, and hydrogen addition reaction was carried out by supplying hydrogen at an initial pressure of 9.1 MPa at 110° C. for 2 hours. After removing a catalyst by filtration, the obtained filtrate was concentrated and dried to obtain 32.4 g of a target compound as a pale red oily product.

1. customat 110° C.
2. customfor 2 hours
3. customAfter removing a catalyst
4. filtrationby filtration
5. concentrationthe obtained filtrate was concentrated
6. customdried