n,n-Bis(2-cyanoethyl)octadecylamine → n,n-Bis(3-aminopropyl)octadecylamine

Participants

Reaction Steps

42.1 g of N,N-bis(2-cyanoethyl)octadecylamine, 3.26 g of RaneyCo, 150 ml of 1,4-dioxane was charged to an autoclave, and hydrogen addition reaction was carried out by supplying hydrogen at an initial pressure of 8.0 MPa at 110° C. for 2 hours. After removing a catalyst by filtration, the obtained filtrate was concentrated and dried to obtain 42.3 g of a target compound as a white solid.

Provenance & Evidence