HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59350552, compound → HCID 59749469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59350552 | HCID 59350552 | — |
| Reactant | HCID 59749517 | HCID 59749517 | — |
| Product | HCID 59749469 | HCID 59749469 | — |
Reaction Steps
Using essentially the same procedure as described for (5R)-5-({[tert-butyl(dimethyl)silyl]oxy}methyl)-3-[4-(trimethylstannyl)phenyl]-1,3-oxazolidin-2-one, but starting from (5R)-5-({[tert-butyl(dimethyl)silyl]oxy}methyl)-3-(3-fluoro-4-iodophenyl)-1,3-oxazolidin-2-one (1.97 g, 4.37 mM) gave the title compound as a white solid after chromatography using hexanes then 20% ethyl acetate/hexanes (1.75 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07396847B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-9d3f4146bed34592b6e31164ced17387 |
| Source note | uspto-grants-2008_07 |