HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl (3-aminopropyl)carbamate → HCID 22350985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl (3-aminopropyl)carbamate | HCID 2735700 | — |
| Reactant | Ethyl 2-Pyridyldithiocarbamate | HCID 12214896 | — |
| Product | HCID 22350985 | HCID 22350985 | 89.7% |
Reaction Steps
In a similar manner to in Reference Example 58, ethyl 2-pyridyldithiocarbamate (1.98 g) and t-butyl 3-aminopropylcarbamate (1.74 g) were reacted and crystallized from n-hexane-diethyl ether to give the title compound (2.78 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07396842B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-603752d31bee4a77bf824cd3c8930a0e |
| Source note | uspto-grants-2008_07 |