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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 747688Generated: October 30, 2026

Hydrochloric Acid → HCID 68833752, compound

https://huagongshe.com/reaction/747688

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 62006965HCID 62006965—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 68833752HCID 68833752—

Reaction Conditions

Temperature95 °C

Reaction Steps

1.28 g (6.60 mmol) of ethyl [N-methyl-N-(pyridine-4-yl)amino]acetate was stirred in 30 ml of dioxane. 26 ml of 1 N hydrochloric acid was added to the resultant mixture, and they were stirred at 95° C. for 20 hours. The solvent was evaporated under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07396844B1
Source datasetuspto-grants-2008_07
ORD IDord-d50aa3187b334e6f9906fff4cd7c8c1d
Source noteuspto-grants-2008_07