HRID747706

反应详情

EQUATION

反应方程式

HRID 747706 的结构方程式

PROCEDURE

实验过程

847 mg (2.43 mmol) of ethyl (1-t-butoxycarbonyl-4-piperidyloxy)benzoate was dissolved in 50 ml of ethanol. 5 ml of 1 N aqueous sodium hydroxide solution was added to the solution, and they were stirred at room temperature for 3 days. The reaction liquid was concentrated and then treated with ethyl acetate as the extractant in an ordinary manner to obtain the title compound.

WORKUP

后处理

  1. customThe reaction liquid
  2. concentrationwas concentrated
  3. additiontreated with ethyl acetate as the extractant in an ordinary manner