HCID 2228055, compound → HCID 20118494, compound

Participants

Reaction Conditions

Reaction Steps

2.32 g (9.12 mmol) of 3-[3-nitrobenzyloxy]benzonitrile and 4.38 g of zinc were suspended in 50 ml of acetic acid, and the obtained suspension was stirred at 45° C. for 4 hours. The insoluble matter was filtered out, and the filtrate was evaporated. 100 ml of chloroform and 50 ml of 1 N aqueous sodium hydroxide solution were added to the residue. After the separation of the liquids followed by the treatment by an ordinary method, the title compound was obtained.

Provenance & Evidence