HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → Acrylic acid hydroxymethyl acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Hydroxymethyl acrylate | HCID 11217233 | — |
| Catalyst | Azobisisobutyronitrile | HCID 6547 | — |
| Solvent | Diethylethylether | HCID 12430074 | — |
| Product | Acrylic acid hydroxymethyl acrylate | HCID 86602181 | 539.3% |
Reaction Steps
To 20 g of tetrahydrofuran (THF) were added 9 g of acrylic acid, 1 g of hydroxymethyl acrylate, and 0.1 g of 2,2′-azobisisobutylronitrile (AIBN). The resulting mixture was reacted at 67° C. for 3 hours. After reaction, the resulting solution was dropped in diethylethyl ether, thereby obtaining 9.2 g of a photoresist polymer of Formula (IVa).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07399570B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-56488cb6f73f4239bade7733aaecf35f |
| Source note | uspto-grants-2008_07 |