HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → Methacrylic acid hydroxypropyl methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 3-Hydroxypropyl methacrylate | HCID 17694 | — |
| Catalyst | Azobisisobutyronitrile | HCID 6547 | — |
| Solvent | Diethylethylether | HCID 12430074 | — |
| Product | Methacrylic acid hydroxypropyl methacrylate | HCID 86602182 | 582.3% |
Reaction Steps
To 20 g of THF were added 9 g of methacrylic acid, 1 g of hydroxypropyl methacrylate, and 0.1 g of AIBN. The resulting mixture was reacted at 67° C. for 3 hours. After reaction, the resulting solution was dropped in diethylethyl ether, thereby obtaining 9.3 g of a photoresist polymer of Formula (IVd).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07399570B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-a4dcbc86eb9c458dae976a088d9d0c1d |
| Source note | uspto-grants-2008_07 |