HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 747958Generated: November 2, 2026
Thionyl Chloride → HCID 59750697, compound
https://huagongshe.com/reaction/747958
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 66673152 | HCID 66673152 | — |
| Product | HCID 59750697 | HCID 59750697 | — |
Reaction Steps
Charge flask with 6-(5-Hydroxy-5,6,7,8-tetrahydro-naphthalen-2-yloxy)-nicotinamide (288 mg, 1.01 mmol) and SOCl2 (5 ml) and heat at 50° C. under nitrogen atmosphere with stirring. After 3.5 hours, concentrate on rotary evaporator to give the title compound as a yellow oil. Due to instability, use this material without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07399774B2 |
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| Source dataset | uspto-grants-2008_07 |
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| ORD ID | ord-eec17b5c93d84b59b49ad83eba02802c |
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| Source note | uspto-grants-2008_07 |
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