Methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoate → HCID 22493640, compound

HRID 748022Notes

Reaction equation

HRID 748022 reaction equation
[OH:1][CH:2]1[CH2:7][CH2:6][CH2:5][CH:4]([O:8][CH2:9][C:10]2[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[C:11]=2[C:12]([O:14]C)=[O:13])[CH2:3]1.[CH3:21][C:22]1[CH:27]=[C:26]([CH3:28])[CH:25]=[CH:24][C:23]=1[C:29]1[O:30][C:31]([CH3:36])=[C:32]([CH2:34]I)[N:33]=1>>[CH3:21][C:22]1[CH:27]=[C:26]([CH3:28])[CH:25]=[CH:24][C:23]=1[C:29]1[O:30][C:31]([CH3:36])=[C:32]([CH2:34][O:1][CH:2]2[CH2:7][CH2:6][CH2:5][CH:4]([O:8][CH2:9][C:10]3[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[C:11]=3[C:12]([OH:14])=[O:13])[CH2:3]2)[N:33]=1

Participants

3

Reactant 2

HCID 21980299Methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoateHCID 22493682HCID 22493682, compound

Product 1

HCID 22493640HCID 22493640, compound

Procedure

Using methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoate and 2-(2,4-dimethylphenyl)-4-iodomethyl-5-methyloxazole as starting materials in the procedure of Example XXXI, gave the product 62 of molecular weight 463.58 (C28H33NO5), MS(ESI): 464.22 (M+H+).

Sources & evidence

ORD record
ord-e7cf64e2e3804c11b52712c873ac9ad5
Source dataset
uspto-grants-2008_07
Patent number
US07399777B2

Reaction notes

Loading…