Methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoate → HCID 22493643, compound

HRID 748023Notes

Reaction equation

HRID 748023 reaction equation
[OH:1][CH:2]1[CH2:7][CH2:6][CH2:5][CH:4]([O:8][CH2:9][C:10]2[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[C:11]=2[C:12]([O:14]C)=[O:13])[CH2:3]1.[CH3:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=1[C:28]1[O:29][C:30]([CH3:35])=[C:31]([CH2:33]I)[N:32]=1>>[CH3:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=1[C:28]1[O:29][C:30]([CH3:35])=[C:31]([CH2:33][O:1][CH:2]2[CH2:7][CH2:6][CH2:5][CH:4]([O:8][CH2:9][C:10]3[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[C:11]=3[C:12]([OH:14])=[O:13])[CH2:3]2)[N:32]=1

Participants

3

Reactant 2

HCID 21980299Methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoateHCID 22493713HCID 22493713, compound

Product 1

HCID 22493643HCID 22493643, compound

Procedure

Using methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoate and 2-(2-methylphenyl)-4-iodomethyl-5-methyloxazole as starting materials in the procedure of Example XXXI, gave the product 63 of molecular weight 449.55 (C27H31NO5), MS(ESI): 450.20 (M+H+).

Sources & evidence

ORD record
ord-4a6c8f8f51f74072960e0ad3aa18661d
Source dataset
uspto-grants-2008_07
Patent number
US07399777B2

Reaction notes

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