Methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoate → HCID 22493665, compound

HRID 748025Notes

Reaction equation

HRID 748025 reaction equation
[OH:1][CH:2]1[CH2:7][CH2:6][CH2:5][CH:4]([O:8][CH2:9][C:10]2[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[C:11]=2[C:12]([O:14]C)=[O:13])[CH2:3]1.[CH3:21][O:22][C:23]1[CH:24]=[C:25]([C:31]2[O:32][C:33]([CH3:38])=[C:34]([CH2:36]I)[N:35]=2)[CH:26]=[CH:27][C:28]=1[O:29][CH3:30]>>[CH3:21][O:22][C:23]1[CH:24]=[C:25]([C:31]2[O:32][C:33]([CH3:38])=[C:34]([CH2:36][O:1][CH:2]3[CH2:7][CH2:6][CH2:5][CH:4]([O:8][CH2:9][C:10]4[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[C:11]=4[C:12]([OH:14])=[O:13])[CH2:3]3)[N:35]=2)[CH:26]=[CH:27][C:28]=1[O:29][CH3:30]

Participants

3

Reactant 2

HCID 21980299Methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoateHCID 22493639HCID 22493639, compound

Product 1

HCID 22493665HCID 22493665, compound

Procedure

Using methyl 2-(3-hydroxycyclohexyloxymethyl)-6-methylbenzoate and 2-(3,4-dimethoxyphenyl)-4-iodomethyl-5-methyloxazol as starting materials in the procedure of Example XXXI, gave the product 67 of molecular weight 495.58 (C28H33NO7), MS(ESI): 496.20 (M+H+).

Sources & evidence

ORD record
ord-d2c2dbaae73d48a78e9733d5ff488abd
Source dataset
uspto-grants-2008_07
Patent number
US07399777B2

Reaction notes

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