Isobutyraldehyde → HCID 68594598, compound

HRID 748053Notes

Reaction equation

HRID 748053 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][CH:10]=[N:9]2)=[CH:4][CH:3]=1.[CH:13](=[O:17])[CH:14]([CH3:16])[CH3:15]>>[CH3:15][CH:14]([CH3:16])[CH:13]([C:12]1[N:8]([C:5]2[CH:4]=[CH:3][C:2]([CH3:1])=[CH:7][CH:6]=2)[N:9]=[CH:10][CH:11]=1)[OH:17]

Participants

3

Reactant 2

HCID 6561IsobutyraldehydeHCID 8097971-p-Tolyl-1H-pyrazole

Product 1

HCID 68594598HCID 68594598, compoundYield 54%

Procedure

This compound was prepared from 1-(4-methylphenyl)-1H-pyrazole (Tetrahedron Lett. 39(19): 2941 (1998)) and isobutyraldehyde using the method described in example 10B and isolated as a clear oil in 54% yield.

Workup

  1. customisolated as a clear oil in 54% yield

Sources & evidence

ORD record
ord-c13915e03c26439d83e6b422e35e649c
Source dataset
uspto-grants-2008_07
Patent number
US07399778B2

Reaction notes

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